1. General information
Course:
APPLIED ANALYTICAL CHEMISTRY
Code:
57331
Type:
ELECTIVE
ECTS credits:
6
Degree:
409 - CHEMISTRY
Academic year:
2023-24
Center:
1 - FACULTY OF SCIENCE AND CHEMICAL TECHNOLOGY
Group(s):
20
Year:
4
Duration:
C2
Main language:
Spanish
Second language:
English
Use of additional languages:
English Friendly:
Y
Web site:
Bilingual:
N
Lecturer:
JOSE MARIA LEMUS GALLEGO
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
FACULTAD DE QUIMICAS
Q. ANALÍTICA Y TGIA. ALIMENTOS
josemaria.lemus@uclm.es
Lecturer:
JOSE ANTONIO MURILLO PULGARIN
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno
Q. ANALÍTICA Y TGIA. ALIMENTOS
3441
joseantonio.murillo@uclm.es
2. Pre-Requisites
Haber aprobado el Módulo de Formación Básica
3. Justification in the curriculum, relation to other subjects and to the profession
The subject of Applied Analytical Chemistry I has optional character in the Degree in Chemistry. The student has already taken the subjects of Fundamentals of Analytical Chemistry and, Volumetric and Gravimetric Analysis and Instrumental Analysis I in the second year in which the foundations of the Analytical Chemistry and the Analytical Process, providing the basic skills and knowledge necessary to face the present subject with guarantees of success. In the third year they study the subjects of Instrumental Analysis II and Instrumental Methods of Separation, compulsory subjects of the third year. This subject studies the application of the main analytical methods supported by the knowledge acquired in the compulsory subjects previously mentioned. It is intended that students develop the necessary skills to be able to solve problems of an analytical nature, that the graduate can be raised in their career
4. Degree competences achieved in this course
| Course competences | |
|---|---|
| Not established. |
5. Objectives or Learning Outcomes
| Course learning outcomes | |
|---|---|
| Not established. | |
| Additional outcomes | |
| Not established. |
6. Units / Contents
-
Unit 1: UNIT 1.- Introduction. Definitions of Analytical Chemistry and Chemical Analysis. Analytical methodology. Stages of the general analytical process. Analytical methods: classification. Importance of chemical analysis.
-
Unit 2: UNIT 2.- Sampling. Basic requirements of sampling. Sampling plan. Conservation and transport of samples. Errors in sampling. Storage of the sample. Preparation of the sample for analysis. Manual of sampling and registration in the laboratory.
-
Unit 3: UNIT 3.- Automatic methods and process analyzers Automatic analysis methods. Classifications Continuous and discontinuous automatic analyzers. Process analyzers Components Photometric, electrochemical and process chromatograph analyzers.
-
Unit 4: UNIT 4. Principles of laboratory management. Standardization. Sections of a norm of analysis. Reference materials: Requirements, preparation, employment and types. Quality control: Basic principles. Quality and traceability Quality assurance plan.
-
Unit 5: UNIT 5.- Introduction to the Environment. Contamination. Atmospheric pollution. The environment and its components. Pollution processes. Air pollutants Sample taking of air and vapors. Analysis of inorganic compounds. Analysis of organic compounds. Determination of particulate material in air.
-
Unit 6: UNIT 6.- Water pollution. Taking and treatment of samples. Physical-chemical and organoleptic characteristics of water. Undesirable and toxic components. Determination of metallic components. Determination of non-metallic inorganic compounds. Determination of organic compounds.
-
Unit 7: UNIT 7.- Soil pollution. Properties of soils and sediments. Interaction of pollutants. Determination of the general characteristics of the soils. Determination of heavy metals. Determination of organic compounds.
-
Unit 8: UNIT 8.- Limestone and siliceous materials. Stony, refractory materials, glasses. Ceramic materials. Minerals Analysis of silicon materials. Analysis of a limestone. Analysis of cements.
-
Unit 9: UNIT 9.- Metallic Materials. Ferrous materials: Steels. Analysis of iron minerals. Analysis of steels. Non-ferrous materials: Brass, bronze and other alloys. Analysis of Bronzes and Brass.
-
Unit 10: UNIT 10.- Coals and derivatives. Classification of Coals and their derivatives. Majority and minority components. Sulfur content. Content in trace elements.
-
Unit 11: UNIT 11.- Petroleum products. Physical and chemical characteristics Specifications for the different fractions. Some determinations in petroleum products: Ashes, traces of water, index of acidity and sulfur.
-
Unit 12: UNIT 12.- Food analysis. Methods and methodologies in Food Science. Basic analysis, acidity of the food and mineral analysis. Analysis in milk and derivatives. Analysis in oils and fats. Analysis in alcoholic drinks. Analysis of additives.
-
Unit 13: UNIT 13.- Pharmaceutical, clinical and toxicological analysis. Identification, characterization and purification of active ingredients. Analytical techniques of separation of active products and their metabolites. Clinical analysis. Toxicological analysis
7. Activities, Units/Modules and Methodology
| Training Activity | Methodology | Related Competences (only degrees before RD 822/2021) | ECTS | Hours | As | Com | Description | |
| Class Attendance (theory) [ON-SITE] | Lectures | 0.9 | 22.5 | N | N | |||
| Class Attendance (practical) [ON-SITE] | Practical or hands-on activities | 0.7 | 17.5 | Y | Y | |||
| Workshops or seminars [ON-SITE] | Guided or supervised work | 0.4 | 10 | Y | N | |||
| Group tutoring sessions [ON-SITE] | Group Work | 0.1 | 2.5 | N | N | |||
| Study and Exam Preparation [OFF-SITE] | Self-study | 1 | 25 | N | N | |||
| Other off-site activity [OFF-SITE] | Project/Problem Based Learning (PBL) | 2.8 | 70 | N | N | |||
| Final test [ON-SITE] | Assessment tests | 0.1 | 2.5 | Y | N | |||
| Total: | 6 | 150 | ||||||
| Total credits of in-class work: 2.2 | Total class time hours: 55 | |||||||
| Total credits of out of class work: 3.8 | Total hours of out of class work: 95 | |||||||
As: Assessable training activity Com: Training activity of compulsory overcoming (It will be essential to overcome both continuous and non-continuous assessment).
8. Evaluation criteria and Grading System
| Evaluation System | Continuous assessment | Non-continuous evaluation * | Description |
| Laboratory sessions | 15.00% | 15.00% | - |
| Theoretical exam | 60.00% | 85.00% | - |
| Projects | 25.00% | 0.00% | - |
| Total: | 100.00% | 100.00% |
According to art. 4 of the UCLM Student Evaluation Regulations, it must be provided to students who cannot regularly attend face-to-face training activities the passing of the subject, having the right (art. 12.2) to be globally graded, in 2 annual calls per subject , an ordinary and an extraordinary one (evaluating 100% of the competences).
Evaluation criteria for the final exam:
-
Continuous assessment:Final numerical rating from 0 to 10 depending on the current legislation.
Continuous evaluation through the acquisition of theoretical knowledge (40%), practical knowledge (laboratory)
(25%) and solving practical cases in the classroom (35%) -
Non-continuous evaluation:Evaluation criteria not defined
Specifications for the resit/retake exam:
Final exam
Specifications for the second resit / retake exam:
Evaluation criteria not defined
9. Assignments, course calendar and important dates
| Not related to the syllabus/contents | |
|---|---|
| Hours | hours |
| Class Attendance (practical) [PRESENCIAL][Practical or hands-on activities] | 17.5 |
| Workshops or seminars [PRESENCIAL][Guided or supervised work] | 10 |
| Group tutoring sessions [PRESENCIAL][Group Work] | 2.5 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 25 |
| Other off-site activity [AUTÓNOMA][Project/Problem Based Learning (PBL)] | 70 |
| Final test [PRESENCIAL][Assessment tests] | 2.5 |
| Unit 1 (de 13): UNIT 1.- Introduction. Definitions of Analytical Chemistry and Chemical Analysis. Analytical methodology. Stages of the general analytical process. Analytical methods: classification. Importance of chemical analysis. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1 |
| Unit 2 (de 13): UNIT 2.- Sampling. Basic requirements of sampling. Sampling plan. Conservation and transport of samples. Errors in sampling. Storage of the sample. Preparation of the sample for analysis. Manual of sampling and registration in the laboratory. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1.5 |
| Unit 3 (de 13): UNIT 3.- Automatic methods and process analyzers Automatic analysis methods. Classifications Continuous and discontinuous automatic analyzers. Process analyzers Components Photometric, electrochemical and process chromatograph analyzers. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1.5 |
| Unit 4 (de 13): UNIT 4. Principles of laboratory management. Standardization. Sections of a norm of analysis. Reference materials: Requirements, preparation, employment and types. Quality control: Basic principles. Quality and traceability Quality assurance plan. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 2.5 |
| Unit 5 (de 13): UNIT 5.- Introduction to the Environment. Contamination. Atmospheric pollution. The environment and its components. Pollution processes. Air pollutants Sample taking of air and vapors. Analysis of inorganic compounds. Analysis of organic compounds. Determination of particulate material in air. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 2.5 |
| Unit 6 (de 13): UNIT 6.- Water pollution. Taking and treatment of samples. Physical-chemical and organoleptic characteristics of water. Undesirable and toxic components. Determination of metallic components. Determination of non-metallic inorganic compounds. Determination of organic compounds. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 2.5 |
| Unit 7 (de 13): UNIT 7.- Soil pollution. Properties of soils and sediments. Interaction of pollutants. Determination of the general characteristics of the soils. Determination of heavy metals. Determination of organic compounds. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1.5 |
| Unit 8 (de 13): UNIT 8.- Limestone and siliceous materials. Stony, refractory materials, glasses. Ceramic materials. Minerals Analysis of silicon materials. Analysis of a limestone. Analysis of cements. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1.5 |
| Unit 9 (de 13): UNIT 9.- Metallic Materials. Ferrous materials: Steels. Analysis of iron minerals. Analysis of steels. Non-ferrous materials: Brass, bronze and other alloys. Analysis of Bronzes and Brass. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1 |
| Unit 10 (de 13): UNIT 10.- Coals and derivatives. Classification of Coals and their derivatives. Majority and minority components. Sulfur content. Content in trace elements. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1 |
| Unit 11 (de 13): UNIT 11.- Petroleum products. Physical and chemical characteristics Specifications for the different fractions. Some determinations in petroleum products: Ashes, traces of water, index of acidity and sulfur. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 1 |
| Unit 12 (de 13): UNIT 12.- Food analysis. Methods and methodologies in Food Science. Basic analysis, acidity of the food and mineral analysis. Analysis in milk and derivatives. Analysis in oils and fats. Analysis in alcoholic drinks. Analysis of additives. | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 2.5 |
| Unit 13 (de 13): UNIT 13.- Pharmaceutical, clinical and toxicological analysis. Identification, characterization and purification of active ingredients. Analytical techniques of separation of active products and their metabolites. Clinical analysis. Toxicological analysis | |
|---|---|
| Activities | Hours |
| Class Attendance (theory) [PRESENCIAL][Lectures] | 2.5 |
| Global activity | |
|---|---|
| Activities | hours |
10. Bibliography and Sources
| Author(s) | Title | Book/Journal | Citv | Publishing house | ISBN | Year | Description | Link | Catálogo biblioteca |
|---|---|---|---|---|---|---|---|---|---|
| Pagina web de Jose Maria Lemus Gallego | 2013 | Archivos de la asignatura | http://www.uclm.es/profesorado/jmlemus/ | ||||||
| APHA (American Public Health Association), AWWA (American Water Works Association), WPCF (Water Pollution Control Federation) | Métodos normalizados para el análisis de aguas potables y residuales | Ed. Diaz de Santos | 1994 | ||||||
| Baird C. | Química Ambiental | Reverté | |||||||
| Boubel R.W., Fox D.L., Turner D.B. y Stern A.C. | Fundamentals of air pollution | Ed. Academic Press. | 1994 | ||||||
| C.Camara | Toma y tratamiento de muestras | Sintesis | 2002 | ||||||
| Developments in food analysis techniques | R.D. King. | London | Applied Science Publishers. | 1978 | |||||
| H.D. Belitz y W. Grosch. | Food Chemistry | Heidelberg | Ed. Spriger-Verlag | 1987 | |||||
| M. Repetto. | Toxicología avanzada | Madrid | Ed. Diaz de Santos | 1995 | |||||
| Miroslav Radojevic and Vladimir N. Bashkin | .Practical Environmental Analysis | Ed. Royal Society of chemistry | 1999 | ||||||
| Pérez-Bendito D. y Rubio S. | Environmental Analytical Chemistry | Elsevier | 1999 | ||||||
| Rodier, J. | Análisis de aguas | Omega | 1989 |