Not established

Not established

Course competences
Code	Description
CB08	Students are able to integrate knowledge and deal with the complexity of making judgements on the basis of incomplete or limited information, including reflections on the social and ethical responsibilities linked to the application of their knowledge and judgements.
CB09	Students are able to communicate their conclusions and the ultimate knowledge and rationale behind them to specialist and non-specialist audiences in a clear and unambiguous way.
CB10	Students possess the learning skills that will enable them to continue studying in a largely self-directed or autonomous way.
CE04	Evaluate the usefulness of separation, analysis and structural determination techniques for joint application in problem solving, and be skilled in the use of such techniques in both research and routine laboratories applying methods of organic and inorganic analysis and/or synthesis.
CE09	To develop experiments that serve as a basis for R+D+I activities in the field of chemistry, facilitating their transfer to the productive world by means of new standardised work procedures validated for routine and/or control laboratories.
CG02	To achieve advanced training in the fundamentals and potential of the instrumental techniques available in chemistry for the development of scientific research and/or application in specialised control laboratories.
CG03	To achieve advanced training in the management and handling of experimental techniques and procedures in the chemical laboratory.

Course learning outcomes
Description
To understand the effect of radiofrequency pulses in NMR.
To know the phenomenon of X-ray diffraction applied to the determination of structures from single crystals or microcrystalline powder.
To know the basis and information provided by RAMAN and IR spectroscopy techniques, especially applied to the study of surfaces.
To understand the rationale and information provided by X-ray spectroscopy techniques (XRF, XANES, EXAFS) and electron spectroscopy (XPS, Auger).
To know the basis and information provided by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and local probe electron microscopy (AFM and STM) techniques. Use of electron microscopy for quantitative analysis (SEM-EDX).
To know the origin of the information conveyed in one- and two-dimensional techniques.
To know the applications of the main one- and two-dimensional pulse sequences.
Handling processing and simulation software for different techniques.
To be able to analyse the information provided by a given technique in order to deduce the structure of the product under study and to know how to select and apply the most appropriate characterisation technique for each type of structural analysis.
To know the main methods of sensitivity transfer
To learn the most advanced NMR techniques, solid resonance, gradients, inverse resonance, imaging, diffusion...
Additional outcomes
Not established.

• Unit 1:
• Unit 2:
• Unit 3:
• Unit 4:
• Unit 5:
• Unit 6:
• Unit 7:
• Unit 8:
• Unit 9:
• Unit 10:
• Unit 11:

Training Activity	Methodology	Related Competences (only degrees before RD 822/2021)	ECTS	Hours	As	Com	Description
Writing of reports or projects [OFF-SITE]	Reading and Analysis of Reviews and Articles	CB08 CB09	1.44	36	Y	Y
Class Attendance (theory) [ON-SITE]	Lectures	CB08 CB09 CB10 CE04 CE09 CG02 CG03	1.2	30	Y	Y
Study and Exam Preparation [OFF-SITE]	Self-study	CB08 CB10 CE04 CG02	1.44	36	Y	N
Analysis of articles and reviews [OFF-SITE]	Self-study	CB08 CB09	1.2	30	Y	Y
Project or Topic Presentations [ON-SITE]	Project/Problem Based Learning (PBL)	CB08 CB09 CB10	0.12	3	Y	N
On-line debates and forums [OFF-SITE]	Cooperative / Collaborative Learning	CB09 CB10 CE04	0.28	7	Y	N
Final test [ON-SITE]	Assessment tests	CB09 CG02	0.08	2	Y	Y
Problem solving and/or case studies [ON-SITE]	Guided or supervised work	CB08 CB09 CB10 CE04 CE09 CG02	0.24	6	Y	Y
Total:			6	150
Total credits of in-class work: 1.64			Total class time hours: 41
Total credits of out of class work: 4.36			Total hours of out of class work: 109

As: Assessable training activity
Com: Training activity of compulsory overcoming (It will be essential to overcome both continuous and non-continuous assessment).

Evaluation System	Continuous assessment	Non-continuous evaluation *	Description
Projects	20.00%	20.00%
Test	40.00%	60.00%
Assessment of problem solving and/or case studies	30.00%	15.00%
Other methods of assessment	5.00%	5.00%
Assessment of active participation	5.00%	0.00%
Total:	100.00%	100.00%

Not related to the syllabus/contents
Hours	hours

Unit 1 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	2
Class Attendance (theory) [PRESENCIAL][Lectures]	2.5
Study and Exam Preparation [AUTÓNOMA][Self-study]	3
Analysis of articles and reviews [AUTÓNOMA][Self-study]	3
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.5
Final test [PRESENCIAL][Assessment tests]	.15

Unit 2 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	1
Class Attendance (theory) [PRESENCIAL][Lectures]	1.5
Study and Exam Preparation [AUTÓNOMA][Self-study]	2
Analysis of articles and reviews [AUTÓNOMA][Self-study]	2
Final test [PRESENCIAL][Assessment tests]	.15

Unit 3 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	4
Class Attendance (theory) [PRESENCIAL][Lectures]	2.5
Study and Exam Preparation [AUTÓNOMA][Self-study]	3
Analysis of articles and reviews [AUTÓNOMA][Self-study]	3
Project or Topic Presentations [PRESENCIAL][Project/Problem Based Learning (PBL)]	1
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.5
Final test [PRESENCIAL][Assessment tests]	.15
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	1

Unit 4 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	5
Class Attendance (theory) [PRESENCIAL][Lectures]	3.5
Study and Exam Preparation [AUTÓNOMA][Self-study]	4
Analysis of articles and reviews [AUTÓNOMA][Self-study]	4
Project or Topic Presentations [PRESENCIAL][Project/Problem Based Learning (PBL)]	1
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	1
Final test [PRESENCIAL][Assessment tests]	.15
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	1

Unit 5 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	2
Class Attendance (theory) [PRESENCIAL][Lectures]	1
Study and Exam Preparation [AUTÓNOMA][Self-study]	1.5
Analysis of articles and reviews [AUTÓNOMA][Self-study]	1
Project or Topic Presentations [PRESENCIAL][Project/Problem Based Learning (PBL)]	1
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.5
Final test [PRESENCIAL][Assessment tests]	.15

Unit 6 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	4
Class Attendance (theory) [PRESENCIAL][Lectures]	4
Study and Exam Preparation [AUTÓNOMA][Self-study]	4.5
Analysis of articles and reviews [AUTÓNOMA][Self-study]	2
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.5
Final test [PRESENCIAL][Assessment tests]	.15
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	.7

Unit 7 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	2.4
Class Attendance (theory) [PRESENCIAL][Lectures]	2
Study and Exam Preparation [AUTÓNOMA][Self-study]	2.4
Analysis of articles and reviews [AUTÓNOMA][Self-study]	2
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.5
Final test [PRESENCIAL][Assessment tests]	.2
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	.2

Unit 8 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	3.6
Class Attendance (theory) [PRESENCIAL][Lectures]	3
Study and Exam Preparation [AUTÓNOMA][Self-study]	3.6
Analysis of articles and reviews [AUTÓNOMA][Self-study]	3
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.8
Final test [PRESENCIAL][Assessment tests]	.2
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	.7

Unit 9 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	3.6
Class Attendance (theory) [PRESENCIAL][Lectures]	3
Study and Exam Preparation [AUTÓNOMA][Self-study]	3.6
Analysis of articles and reviews [AUTÓNOMA][Self-study]	3
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.8
Final test [PRESENCIAL][Assessment tests]	.2
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	.7

Unit 10 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	1.2
Class Attendance (theory) [PRESENCIAL][Lectures]	1
Study and Exam Preparation [AUTÓNOMA][Self-study]	1.2
Analysis of articles and reviews [AUTÓNOMA][Self-study]	1
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	.4
Final test [PRESENCIAL][Assessment tests]	.1
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	.2

Unit 11 (de 11):
Activities	Hours
Writing of reports or projects [AUTÓNOMA][Reading and Analysis of Reviews and Articles]	7.2
Class Attendance (theory) [PRESENCIAL][Lectures]	6
Study and Exam Preparation [AUTÓNOMA][Self-study]	7.2
Analysis of articles and reviews [AUTÓNOMA][Self-study]	6
On-line debates and forums [AUTÓNOMA][Cooperative / Collaborative Learning]	1.5
Final test [PRESENCIAL][Assessment tests]	.4
Problem solving and/or case studies [PRESENCIAL][Guided or supervised work]	1.5

Global activity
Activities	hours

Author(s)	Title	Book/Journal	Citv	Publishing house	ISBN	Year	Description	Link	Catálogo biblioteca
A. K. Cheetham, P. Day	Solid State Chemistry. Thecniques	Libro	Oxford	Oxford University Press	0-19-855165-7	1991	Incluye la mayoría de las técnicas vistas en la asignatura, en algunos caos a un nivel más elevado	https://onlinelibrary.wiley.com/doi/10.1002/qua.560340110
A. R. West	Basic Solid State Chemistry	Libro		WILEY	0-471-91798-2	1984	Libro básico de Química del estado sólido pero que incluye también técnicas de caracterización	https://onlinelibrary.wiley.com/doi/abs/10.1002/%28SICI%291099-0739%28200004%2914%3A4%3C227%3A%3AAID-AOC949%3E3.0.CO%3B2-F
G. Ertl	Reaction at Solid Surfaces	Libro	Hoboken	Wiley	9780470535295	2009	Estudio detallado de las superficies de sólidos y reacciones sobre ellas	https://onlinelibrary.wiley.com/doi/book/10.1002/9780470535295
H. Friebolin	Basic One- and Two Dimensional NMR Spectroscopy	Libro	Manheim	WILEY	978-3-527-32782-9	2010	Texto básico y muy didaction sobre RMN en una y dos dimensiones	https://www.wiley.com/en-us/Basic+One+and+Two+Dimensional+NMR+Spectroscopy%2C+5th%2C+Completely+Revised+and+Updated+Edition-p-9783527327829
H. Günther	NMR Spectroscopy	Libro	Weinheim	WILEY	978-3-527-33004-1	2013	Libro avanzado de RMN con bastantes aspectos teóricos	https://www.wiley.com/en-us/NMR+Spectroscopy%3A+Basic+Principles%2C+Concepts+and+Applications+in+Chemistry%2C+3rd+Edition-p-9783527330003
J. C. Vickerman, I. S. Gimore, Eds.	Surface Analysis. The Principal Techniques	Libro	Chichester	Wiley	9780470017630	2009	Libro sobre diferentes técnicas de caracterización de superficies. Muy bueno el capítulo de XPS	https://www.wiley.com/en-us/Surface+Analysis%3A+The+Principal+Techniques%2C+2nd+Edition-p-9780470017630
J. M. Albella, A. M. Cintas, T. Miranda, J. M. Serratosa	Introducción a la Ciencia de materiales. Técnicas de preparación y caracterización	Libro	Madrid	CSIC	84-00-07343-6	1993	Libro de ciencia de materiales. Incluye técnicas de rayos X, de microscopia electrónica y esp. vibracional.
J. M. Thomas, W. J. Thomas	Principles and Practice of Heterogeneous Catalysis	Libro	Weinheim	VCH	3-527-29239-X	1997	Libro sobre catálisis heterogénea. Incluye un capitulo de caracterización de las superficies de catalizadores, con muchas técnicas a un nivel relativamente básico.	https://onlinelibrary.wiley.com/doi/abs/10.1002/bbpc.199700023
Jenny P. Glusker; Mitchell Lewis and Miriam Rossi	Crystal Structure Analysis for Chemists and Biologists	Libro		VCH	0-89573-273-4	1994		https://onlinelibrary.wiley.com/doi/abs/10.1002/crat.2170310212
M. Martínez-Ripoll, F. Hernández-Cano	Cristalografía			WILEY		2016	Una buena parte de los contenidos se encuentran también en: http://www.xtal.iqfr.csic.es/Cristalografia/	https://www.xtal.iqfr.csic.es/Cristalografia/index.html
R. Freeman	Magnetic Resonance in Chemistry and Medicine	Libro	Oxford	Oxford University Press	0-19-926225-X	2005	libro práctico y didáctico que enlaza la RMN clásica y la imagen por RMN	https://global.oup.com/academic/product/magnetic-resonance-in-chemistry-and-medicine-9780199262250?cc=es&lang=en&
S. Berger, S. Braun	200 and More NMR Experiments: A Practical Course	Libro	Weinheim	VCH	978-3-527-31067-8	2004	Libro práctico sobre secuencias de pulso mono y bidimensionales	https://www.wiley.com/en-us/200+and+More+NMR+Experiments%3A+A+Practical+Course-p-9783527310678
S. L. Flegler, J. W. Heckman, Jr., Klomparens, K. L.	Scanning and Transmission Electron Microscopy. An Introduction	Libro		Oxford University Press		1993	Libro que profundiza en las técnicas de SEM y TEM y en mic. electrónica par análisis