Guías Docentes Electrónicas
1. General information
Course:
LABORATORY BASIC OPERATIONS
Code:
57305
Type:
BASIC
ECTS credits:
6
Degree:
409 - CHEMISTRY
Academic year:
2022-23
Center:
1 - FACULTY OF SCIENCE AND CHEMICAL TECHNOLOGY
Group(s):
20  23 
Year:
1
Duration:
C2
Main language:
Spanish
Second language:
Use of additional languages:
English Friendly:
Y
Web site:
Bilingual:
N
Lecturer: AURELIA ALAÑON MOLINA - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
San Alberto Magno/planta baja
Q. ANALÍTICA Y TGIA. ALIMENTOS
6702
aurelia.alanon@uclm.es

Lecturer: ALFONSO ARANDA RUBIO - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Marie Curie/2ª planta
QUÍMICA FÍSICA
3484
alfonso.aranda@uclm.es
Tuesday, Wednesday and Thursday. 12-14h

Lecturer: BEATRIZ CABAÑAS GALAN - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Edificio Marie Curie (primer piso)
QUÍMICA FÍSICA
6239
beatriz.cabanas@uclm.es
monday 12 to 14h, friday 10 to 12 h and tuesday 16 to 18h

Lecturer: AGUSTIN LARA SANCHEZ - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno
QUÍMICA INORG., ORG., Y BIOQ.
3499
agustin.lara@uclm.es
Tuesday and Thursday from 17:00 to 19:00 h.

Lecturer: MARIA REYES LOPEZ ALAÑON - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Marie Curie (segunda planta))
QUÍMICA FÍSICA
3453
reyes.lopez@uclm.es
Tuesday and Wednesday: 10-12 h Thursday: 17-19 h

Lecturer: Mª ISABEL LOPEZ SOLERA - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno (primer piso)
QUÍMICA INORG., ORG., Y BIOQ.
6282
mabel.lopez@uclm.es
Monday, Wednesday and Friday: 12 - 14 h

Lecturer: JUANA RODRIGUEZ FLORES - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
S. Alberto Magno
Q. ANALÍTICA Y TGIA. ALIMENTOS
3444
juana.rflores@uclm.es
TUESDAY AND WEDNESDAY FROM 16 TO 19

Lecturer: MARIA DEL PRADO SANCHEZ VERDU - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
S. Alberto Magno, 2ª planta
QUÍMICA INORG., ORG., Y BIOQ.
3465
mariaprado.sanchez@uclm.es
tuesday and wednesday from 11 a.m. to 1 p.m.

Lecturer: ANA SANCHEZ-MIGALLON BERMEJO - Group(s): 20  23 
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno
QUÍMICA INORG., ORG., Y BIOQ.
3407
ana.smigallon@uclm.es
Monday from 12:00 to 14:00

2. Pre-Requisites

There are no prerequisites for this subject although it is recommended that the student has studied chemistry in high school. It is advisable that the student is taking the subject of Fundamentals of Chemistry

3. Justification in the curriculum, relation to other subjects and to the profession

Basic Laboratory Operations, is a fundamentally experimental subject. In this subject it is intended that the student acquires good working practices in a laboratory, manipulating with responsibility and security the chemical products; he will begin to know the material, the instrumentation and the basic operations of a laboratory through a series of practical activities. Likewise, they will acquire the necessary skills to be able to correctly develop the practical experiments that will be required in other subjects of the curriculum and in their future professional life.


4. Degree competences achieved in this course
Course competences
Code Description
CB01 Prove that they have acquired and understood knowledge in a subject area that derives from general secondary education and is appropriate to a level based on advanced course books, and includes updated and cutting-edge aspects of their field of knowledge.
CB03 Be able to gather and process relevant information (usually within their subject area) to give opinions, including reflections on relevant social, scientific or ethical issues.
E01 Understand and use chemical terminology, nomenclature, conventions and units
E02 Deduce the variation of the properties of the chemical elements according to the Periodic Table
E03 Handle chemicals safely and with respect to the environment
E07 Relate macroscopic properties with those of atoms, molecules and non-molecular chemical compounds
E15 Know how to handle the standard chemical instrumentation and be able to elaborate and manage standardized procedures of work in the laboratory and chemical industry
G01 Know the principles and theories of Chemistry, as well as the methodologies and applications characteristic of analytical chemistry, physical chemistry, inorganic chemistry and organic chemistry, understanding the physical and mathematical bases that require
G02 Be able to gather and interpret data, information and relevant results, obtain conclusions and issue reasoned reports on scientific, technological or other problems that require the use of chemical tools
T03 Proper oral and written communication
T05 Organization and planning capacity
5. Objectives or Learning Outcomes
Course learning outcomes
Description
Encourage and promote in the student all those values ¿¿and attitudes inherent to scientific activity.
Know the basic concepts and principles of Chemistry, so that the essential foundations are established so that they can successfully face the study of the different branches of the discipline.
Homogenize the knowledge of Chemistry already acquired by students in Secondary School courses and complete certain aspects that have not been previously studied with the necessary depth.
Achieve that the student acquires the basic terminology of Chemistry and knows how to use it, as well as being able to establish relationships between the different concepts.
Know and correctly handle the different units.
Learn to work autonomously in a laboratory and know how to interpret the experimental results obtained.
Additional outcomes
Description
Handle and treat properly chemical reagents and their residues.
Learn the handling of laboratory material as well as different basic measuring instruments in a chemical laboratory.
Learn how to write a laboratory notebook and prepare a report on the activities carried out and the results obtained.
Skillfully perform basic laboratory operations
Knowing and complying with safety regulations in a laboratory.
6. Units / Contents
  • Unit 1: Security and waste management
  • Unit 2: Experimental introduction to basic chemical laboratory techniques
  • Unit 3: Laboratory material handling
  • Unit 4: Obtaining and analyzing results
  • Unit 5: Management of bibliographic search databases, calculation and presentation programs
ADDITIONAL COMMENTS, REMARKS

The contents of the course will be developed through a series of practical activities in which the different aspects and basic laboratory operations will be worked on.


7. Activities, Units/Modules and Methodology
Training Activity Methodology Related Competences ECTS Hours As Com Description
Laboratory practice or sessions [ON-SITE] Practical or hands-on activities CB01 CB03 E01 E02 E03 E07 E15 G01 G02 T03 T05 2.56 64 Y Y Practical activities in which the different aspects and basic laboratory operations will be worked on. As it is an experimental activity of compulsory and not recoverable (according to Art. 4.3.f of the student's evaluation regulations) the realization of the practices will be compulsory in accordance with the official program of the subject.
Practicum and practical activities report writing or preparation [OFF-SITE] Guided or supervised work CB01 CB03 E01 G01 G02 T03 1.28 32 Y Y Creation of the workbook and related issues
Study and Exam Preparation [OFF-SITE] Self-study CB01 CB03 E01 G01 G02 T05 1.6 40 N N Autonomous work of the student to reach the competences
Final test [ON-SITE] Assessment tests CB01 CB03 E01 G01 G02 T03 T05 0.08 2 Y Y Written final evaluation test
Group tutoring sessions [ON-SITE] Group tutoring sessions E01 E03 E07 G01 G02 0.48 12 N N Resolution of doubts
Total: 6 150
Total credits of in-class work: 3.12 Total class time hours: 78
Total credits of out of class work: 2.88 Total hours of out of class work: 72

As: Assessable training activity
Com: Training activity of compulsory overcoming (It will be essential to overcome both continuous and non-continuous assessment).

8. Evaluation criteria and Grading System
Evaluation System Continuous assessment Non-continuous evaluation * Description
Laboratory sessions 60.00% 60.00% Personal work in the laboratory will be evaluated: preparation of activities, order, cleanliness, compliance with safety standards, preparation of the laboratory notebook, carrying out calculations, carrying out practices, obtaining data and discussing results.
Final test 40.00% 40.00% There will be a theoretical-practical exam on the activities carried out in the laboratory.
Total: 100.00% 100.00%  
According to art. 6 of the UCLM Student Evaluation Regulations, it must be provided to students who cannot regularly attend face-to-face training activities the passing of the subject, having the right (art. 13.2) to be globally graded, in 2 annual calls per subject , an ordinary and an extraordinary one (evaluating 100% of the competences).

Evaluation criteria for the final exam:
  • Continuous assessment:
    The course will be passed when a minimum grade of 5.0 is obtained. It will be necessary to obtain a minimum grade of 4.0 in the final exam in order to average with the programmed activities.
  • Non-continuous evaluation:
    The same criteria of the continuous evaluation are maintained, considering that the course includes practical activities of obligatory and not recoverable overcoming according to Art. 4.3.f of the student's evaluation regulations.

Specifications for the resit/retake exam:
The same criteria of the ordinary evaluation are maintained.
Specifications for the second resit / retake exam:
There will be a laboratory and content exam of the programmed practices, provided that the student has completed and passed the practical laboratory activities.
9. Assignments, course calendar and important dates
Not related to the syllabus/contents
Hours hours
Practicum and practical activities report writing or preparation [AUTÓNOMA][Guided or supervised work] 32
Study and Exam Preparation [AUTÓNOMA][Self-study] 40
Final test [PRESENCIAL][Assessment tests] 2

Unit 1 (de 5): Security and waste management
Teaching period: 16-01-23 to 8-02-23
Group 20:
Initial date: 16-01-2023 End date: 19-01-2023
Group 23:
Initial date: 20-01-2023 End date: 08-02-2023
Comment: PREPARATION OF SOLUTIONS Laboratory practicals [PRESENT] [Practical] 5 h STANDARDIZATION OF SOLUTIONS. ACID-BASE TITRATIONS. Laboratory practicals [PRESENT] [Practical] 5 h REACTIONS IN TEST TUBE Laboratory practices [PRESENT] [Practical] 5 h FILTRATION AND CRYSTALLIZATION TECHNIQUES. Laboratory practices [PRESENT] [Practical] 10 h QUALITATIVE ANALYSIS OF IONS. Laboratory practicals [PRESENT][Practical] 5 h EXTRACTION TECHNIQUES. Laboratory practices [PRESENT][Practical] 5 h SUBLIMATION Laboratory practicals [PRESENT] [Practical] 5 h SIMPLE AND FRACTIONAL DISTILLATION Laboratory practicals [PRESENT] [Practical] 5 h VACUUM DISTILLATION Laboratory practical [PRESENT] [Practical] 5 h DETERMINATION OF MELTING POINTS Laboratory practical [PRESENT] [Practical] 5 h THIN LAYER CHROMATOGRAPHY Laboratory practical [PRESENT] [Practical] 5 h CHEMICAL KINETICS Laboratory practicals [PRESENT] [Practical] 5 h ELECTROCHEMISTRY: VOLTAIC PILE Laboratory practice [PRESENT] [Practical] 5 h

Global activity
Activities hours
General comments about the planning: Consult the weekly timetable of the course and the internship calendar published on the Virtual Campus.
10. Bibliography and Sources
Author(s) Title Book/Journal Citv Publishing house ISBN Year Description Link Catálogo biblioteca
 
 
Hill, Graham Chemistry in context: laboratory manual Nelson Thornes 0-17-448307-4 2001 Ficha de la biblioteca
J. Martínez Urrega y col. Experimentación en química general Thomson 84-9732-425-0 2006 Ficha de la biblioteca
M.J. Rodríguez Yunta, F. G. Curso experimental en Química Orgánica Síntesis 2008  
Petrucci, Ralph H. General chemistry: principles and modern applications Prentice Hall 0-13-014329-4 2002 Ficha de la biblioteca
Petrucci, Ralph H. Química general Pearson-Prentice Hall 978-84-205-3533-3 2010 Ficha de la biblioteca
Petrucci-Harwood-Hearing Química General  
Szafran, Zvi Microscale general chemistry laboratory: with selected macro John Wiley & Sons 0-471-62114-5 1993 Ficha de la biblioteca
V. Semishi Prácticas de Química General Inorgánica MIR 2009  



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