1. General information
Course:
ADVANCED LABORATORY IN INSTRUMENTAL TECHNIQUES
Code:
311124
Type:
CORE COURSE
ECTS credits:
6
Degree:
2366 - MASTER DEGREE PROGRAMME IN CHEMICAL
Academic year:
2023-24
Center:
1 - FACULTY OF SCIENCE AND CHEMICAL TECHNOLOGY
Group(s):
20
Year:
1
Duration:
C2
Main language:
Spanish
Second language:
English
Use of additional languages:
English Friendly:
Y
Web site:
Bilingual:
N
Lecturer:
YOLANDA DIAZ DE MERA MORALES
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Edificio Marie Curie, segunda planta, despacho 2.05
QUÍMICA FÍSICA
926052872
yolanda.diaz@uclm.es
Monday and Wednesday: from 16:00h to 18:00h Tuesday and Thursday: from 12:00h to 13:00h
Lecturer:
GEMA DURA GRACIA
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno (primer piso)
QUÍMICA INORG., ORG., Y BIOQ.
Gema.Dura@uclm.es
Monday Tuesday and Wednesday from 16-18 hours
Lecturer:
ANTONIO DE LA HOZ AYUSO
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
San Alberto Magno
QUÍMICA INORG., ORG., Y BIOQ.
926295411
antonio.hoz@uclm.es
Monday, Tuesday and Thursday from 16.00 to 18.00 h
Lecturer:
FELIX ANGEL JALON SOTES
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
San Alberto Magno/Planta primera
QUÍMICA INORG., ORG., Y BIOQ.
926052184
felix.jalon@uclm.es
Monday, Tuesday and Wednesday from 5:00 p.m. to 7:00 p.m.
Lecturer:
ELENA JIMENEZ MARTINEZ
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
EDIFICIO MARIE CURIE, 2ª PLANTA
QUÍMICA FÍSICA
926052129
elena.jimenez@uclm.es
Mon-Tues-Wends: 13:00-14:00 and 16:00-17:00
Lecturer:
MARIA DEL PILAR MARTIN PORRERO
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Marie Curie, 2ª planta
QUÍMICA FÍSICA
926052614
mariapilar.martin@uclm.es
Monday from 11 to 13, Wednesday and Thursday from 16 to 18
Lecturer:
JOSE ANTONIO MURILLO PULGARIN
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Edificio San Alberto Magno
Q. ANALÍTICA Y TGIA. ALIMENTOS
3441
joseantonio.murillo@uclm.es
Lecturer:
ANA MARIA RODRIGUEZ FERNANDEZ-PACHECO
- Group(s):
20
Building/Office
Department
Phone number
Email
Office hours
Politécnico/A23
QUÍMICA INORG., ORG., Y BIOQ.
926051961
anamaria.rfdez@uclm.es
Monday, Tuesday and Wednesday from 4:30 p.m. to 6:30 p.m.
2. Pre-Requisites
Those established for admission to the Master
3. Justification in the curriculum, relation to other subjects and to the profession
The Advanced Laboratory in Instrumental Techniques subject represents the practical part of the Advanced Structural Characterization Techniques and Advanced Instrumental Analysis Techniques subjects. Chemistry is not understood without a practical component and in this sense this subject brings together the real use of the instrumentation that is studied in the aforementioned subjects.
4. Degree competences achieved in this course
| Course competences | |
|---|---|
| Code | Description |
| CB09 | Students are able to communicate their conclusions and the ultimate knowledge and rationale behind them to specialist and non-specialist audiences in a clear and unambiguous way. |
| CB10 | Students possess the learning skills that will enable them to continue studying in a largely self-directed or autonomous way. |
| CE04 | Evaluate the usefulness of separation, analysis and structural determination techniques for joint application in problem solving, and be skilled in the use of such techniques in both research and routine laboratories applying methods of organic and inorganic analysis and/or synthesis. |
| CE07 | To learn about the possibilities offered by new analytical methodologies in different fields of application, as well as the current trends in analytical chemistry of interest for the development of R+D+I or its implementation in specialised control laboratories. |
| CE09 | To develop experiments that serve as a basis for R+D+I activities in the field of chemistry, facilitating their transfer to the productive world by means of new standardised work procedures validated for routine and/or control laboratories. |
| CG01 | Transfer the concepts and fundamentals of chemistry in the context of scientific research and/or in the specialised profession of the chemist. |
| CG02 | To achieve advanced training in the fundamentals and potential of the instrumental techniques available in chemistry for the development of scientific research and/or application in specialised control laboratories. |
| CG03 | To achieve advanced training in the management and handling of experimental techniques and procedures in the chemical laboratory. |
5. Objectives or Learning Outcomes
| Course learning outcomes | |
|---|---|
| Description | |
| To know how to design and implement standardised procedures with instrumental techniques involving the development of validated methods of analysis and/or chemical characterisation characteristic of advanced methodological development. | |
| Knowing how to strategically process data and interpret results involving advanced tools of metrology, chemometrics and qualimetry. | |
| Knowing how to select, use and adapt, if necessary, the different instrumental techniques for the resolution of specific chemical problems. | |
| Additional outcomes | |
| Not established. |
6. Units / Contents
-
Unit 1: Chosen Technique 1 (see comments)
-
Unit 2: Chosen Technique 2 (see comments)
-
Unit 3: Chosen Technique 3 (see comments)
-
Unit 4: Chosen Technique 4 (see comments)
-
Unit 5: Chosen Technique 5 (see comments)
-
Unit 6: Chosen Technique 6 (see comments)
-
Unit 7: Instrumental techniques in a specific research laboratory or in a company
ADDITIONAL COMMENTS, REMARKS
In order to adquire for the student the appropriate profile for their specialization, they must take 6 of the techniques listed below. The choice of techniques that outline your specialization must have the approval of your tutor and may be modified in part for academic reasons by the Master's Academic Committee.
Techniques offered:
-Single Crystal RX Diffraction
-Diffraction RX of powder
-Electron microscopy SEM
-Atomic Force Microscopy (AFM)
-Chemical analysis by XRF
-Thermal analysis: DSC, TGA and heating microscopy
-Particle size: Pycnometry of He, Sedigraph.
-Physical adsorption of gases
-MALDI-TOF mass spectrometry
-FTIR sampling techniques: diffuse reflectance (DRIFTS)
- FTIR spectroscopy with multipass absorption system for the study of processes in gas phases
- Gas chromatography with coupled triple quadrupole spectrometer (GC-MS)
- Gas Chromatography with Time of Flight Mass Spectrometer. Electron Impact (EI) and Field Ionization (FD) (GC-TOFMS)
- Laser induced fluorescence (LIF)
- Proton Transfer Ionization Time of Flight Mass Spectrometry (PTR-ToF-MS)
- Nuclear Magnetic Resonance Spectroscopy in one and two dimensions (including dynamic resonance)
- Study of Vis-UV and fluorescence spectra of molecular compounds in solution
- Estimation of lifetime in excited state of fluorescent and phosphorescent molecules
Topic 7 will be carried out in a specific research group or in a company
7. Activities, Units/Modules and Methodology
| Training Activity | Methodology | Related Competences (only degrees before RD 822/2021) | ECTS | Hours | As | Com | Description | |
| Class Attendance (practical) [ON-SITE] | Guided or supervised work | CE04 CE07 CE09 CG01 CG02 CG03 | 3.84 | 96 | Y | Y | ||
| Study and Exam Preparation [OFF-SITE] | Self-study | CB10 | 0.64 | 16 | N | N | ||
| Analysis of articles and reviews [OFF-SITE] | Reading and Analysis of Reviews and Articles | CB10 CE07 CE09 CG01 CG02 | 0.64 | 16 | N | N | ||
| Writing of reports or projects [OFF-SITE] | Individual presentation of projects and reports | CB09 CG01 | 0.4 | 10 | Y | Y | ||
| On-line debates and forums [OFF-SITE] | Online Forums | CB09 CG01 | 0.2 | 5 | N | N | ||
| Study and Exam Preparation [OFF-SITE] | Assessment tests | CB09 CB10 CE04 CE07 CG01 CG02 CG03 | 0.08 | 2 | N | N | ||
| Individual tutoring sessions [ON-SITE] | Guided or supervised work | CB09 CB10 CE04 CE07 CE09 CG01 CG02 CG03 | 0.2 | 5 | N | N | ||
| Total: | 6 | 150 | ||||||
| Total credits of in-class work: 4.04 | Total class time hours: 101 | |||||||
| Total credits of out of class work: 1.96 | Total hours of out of class work: 49 | |||||||
As: Assessable training activity Com: Training activity of compulsory overcoming (It will be essential to overcome both continuous and non-continuous assessment).
8. Evaluation criteria and Grading System
| Evaluation System | Continuous assessment | Non-continuous evaluation * | Description |
| Practicum and practical activities reports assessment | 80.00% | 80.00% | 80% will consist of a report of the practices carried out. |
| Other methods of assessment | 10.00% | 10.00% | On-line activities of the techniques, for example a pre-laboratory questionnaire |
| Final test | 10.00% | 10.00% | It will consist of an oral and compulsory presentation of the practical case studied |
| Total: | 100.00% | 100.00% |
According to art. 4 of the UCLM Student Evaluation Regulations, it must be provided to students who cannot regularly attend face-to-face training activities the passing of the subject, having the right (art. 12.2) to be globally graded, in 2 annual calls per subject , an ordinary and an extraordinary one (evaluating 100% of the competences).
Evaluation criteria for the final exam:
-
Continuous assessment:Attendance at practical sessions is compulsory.
Each evaluation test must reach the minimum score of 4 points to pass the subject, which after weighing all the tests must reach the minimum score of 5.
The oral presentation of one or two practices is mandatory -
Non-continuous evaluation:Attendance at practical sessions is compulsory.
The oral presentation of one or two practices is mandatory
Same criteria as continuous evaluation.
Specifications for the resit/retake exam:
The qualification of those parts in which more than 4 points have been reached can be saved and those in which it has not been reached must be recovered to obtain the minimum average of 5 points.
Specifications for the second resit / retake exam:
Evaluation criteria not defined
9. Assignments, course calendar and important dates
| Not related to the syllabus/contents | |
|---|---|
| Hours | hours |
| Unit 1 (de 7): Chosen Technique 1 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 2 (de 7): Chosen Technique 2 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 3 (de 7): Chosen Technique 3 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 4 (de 7): Chosen Technique 4 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 5 (de 7): Chosen Technique 5 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 6 (de 7): Chosen Technique 6 (see comments) | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 8 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 1.33 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 1.33 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | .83 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | .42 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | .17 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | .42 |
| Unit 7 (de 7): Instrumental techniques in a specific research laboratory or in a company | |
|---|---|
| Activities | Hours |
| Class Attendance (practical) [PRESENCIAL][Guided or supervised work] | 48 |
| Study and Exam Preparation [AUTÓNOMA][Self-study] | 8 |
| Analysis of articles and reviews [AUTÓNOMA][Reading and Analysis of Reviews and Articles] | 8 |
| Writing of reports or projects [AUTÓNOMA][Individual presentation of projects and reports] | 5 |
| On-line debates and forums [AUTÓNOMA][Online Forums] | 2.5 |
| Study and Exam Preparation [AUTÓNOMA][Assessment tests] | 1 |
| Individual tutoring sessions [PRESENCIAL][Guided or supervised work] | 2.5 |
| Global activity | |
|---|---|
| Activities | hours |
10. Bibliography and Sources
| Author(s) | Title | Book/Journal | Citv | Publishing house | ISBN | Year | Description | Link | Catálogo biblioteca |
|---|---|---|---|---|---|---|---|---|---|
| A. K.Cheetham and Peter Day | Solid State Chemistry: techniques | Libro | Oxford | Oxford Science publications | 0-19-855286-6 | 2001 | ibro de consulta específico | https://catalogobiblioteca.uclm.es/cgi-bin/abnetopac/O7682/IDbed4c285/NT1 | |
| Edmond de Hoffmann y Vicent Stroobant | Mass Spectrometry. Principles and Applications | Libro | Wiley and Sons | 1118681940, 97811186 | 2013 | ||||
| Gross, J | Gross, J Mass Spectrometry: a textbook | Libro | Springer International Publishing | 3319543970, 97833195 | 2017 | ||||
| Helmut H. Telle, Ángel González Ureña | Laser Spectroscopy and Laser Imaging | Libro | CRC Press | 9781315156989 | 2017 | https://doi.org/10.1201/9781315156989 | |||
| J.A. Murillo Pulgarín, A. Alañón Molina and F. Martínez Ferreras | Simultaneous determination of nabumetone and its princuipal metabolite in medicines and human urine by time-resolved fluorescence | Revista | Analyst 137(2012)5144-5152 | 2012 | https://pubs.rsc.org/en/content/articlelanding/2012/an/c2an35412h#!divAbstract | ||||
| Martín Martínez-Ripoll; | Cristalografía | enlace web | Madrid | http://www.xtal.iqfr.csic.es/Cristalografia/ | |||||
| Stefan Berger, Siegmar Braun | 200 and More NMR Experiments: A Practical Course | Libro | Weinheim | Wiley | ISBN: 978-3-527-3106 | 2004 | Libro práctico sobre secuencias de pulso y aplicaciones | https://www.wiley.com/en-us/200+and+More+NMR+Experiments%3A+A+Practical+Course-p-9783527310678 | |
| West , A. R. | Basic Solid State Chemistry | Libro | New York | John Wiley and Sons | 0-471-98755-7 | 1999 | Libro de consulta específico | https://catalogobiblioteca.uclm.es/cgi-bin/abnetopac/O7682/IDbed4c285/NT1 |