No prerequisites have been established, although it is very recommended to have passed the first-year Chemistry course.

Gravimetric and Volumetric Analysis is a subject that belongs to module 2 (Fundamentals of Chemistry). This subject and Fundamental of Analytical Chemistry constitute Analytical Chemical Matter which has 12 credits. Both of them are taught in the first semester of the second year.

It is a compulsory subjectof 6 ECTS (4.5 theoretical credits and 1.5 practical credits). Furthermore, the knowledge acquired in this subject is necessary to learn subjects from other areas of knowledge, due to its multidisciplinary character

Course competences
Code	Description
CB02	Apply their knowledge to their job or vocation in a professional manner and show that they have the competences to construct and justify arguments and solve problems within their subject area.
CB03	Be able to gather and process relevant information (usually within their subject area) to give opinions, including reflections on relevant social, scientific or ethical issues.
CB05	Have developed the necessary learning abilities to carry on studying autonomously
E05	Know the chemical elements and their compounds, their forms of obtaining, structure, properties and reactivity, as well as the main techniques for their analysis
E14	Know and know how to apply the metrology of chemical processes, including quality management
E15	Know how to handle the standard chemical instrumentation and be able to elaborate and manage standardized procedures of work in the laboratory and chemical industry
G01	Know the principles and theories of Chemistry, as well as the methodologies and applications characteristic of analytical chemistry, physical chemistry, inorganic chemistry and organic chemistry, understanding the physical and mathematical bases that require
G03	Know how to apply the theoretical-practical knowledge acquired in the different professional contexts of Chemistry
T04	Ethical commitment and professional ethics
T05	Organization and planning capacity
T06	Ability to approach decision making
T09	Motivation for quality, job security and awareness of environmental issues, with knowledge of internationally recognized systems for the correct management of these aspects
T11	Ability to obtain bibliographic information, including Internet resources

Course learning outcomes
Description
Acquire skills for practical laboratory work, being able to experimentally develop analytical processes that include sample planning, treatment and analysis using volumetric and gravimetric techniques.
Train the student for autonomous work and learning, as well as for personal initiative
Train the student to search for information, its analysis, interpretation and use for analytical purposes
Train the student to be sensitive to the ethical exercise of the profession, becoming aware of the social responsibility of their reports and their impact on decision making
Train the student to solve analytical problems based on the use of volumetric and gravimetric analysis techniques, planning laboratory work protocols.
Know the basis of volumetric and gravimetric techniques and the main analytical methods based on these techniques.
Know the stages that make up the analytical process
Know the principles of Analytical Chemistry.
Additional outcomes
Not established.

• Unit 1: INTRODUCTION. Classical techniques: Gravimetry and Titrimetry. Classification of volumetric methods. Primary standards
• Unit 2: ACID- BASE TITRATIONS. Acid-base Indicators. Types of indicators. Titration curves: Titration of monoprotic and polyprotic protolytes. Analytical applications.
• Unit 3: COMPLEXATION TITRATIONS. Complexation reactions. Titration curves. Complexometric EDTA Titrations. Metallochromic indicators. Types of complexation titration. Applications.
• Unit 4: PRECIPITATION TITRATIONS. Introduction. Titration Curves. Mohr¿ method. Volhard¿ method. Fajans¿ method. Most used primary standards
• Unit 5: Gravimetry. Introduction. Types of gravimetric methods. Formation and treatment of precipitates. Precipitation gravimetry. General steps involved in gravimetric analysis.
• Unit 6: REDOX TITRATIONS. Titration Curves. Redox indicators. Pre-treatment in redox titrations. Titrations with permanganate. Titrations with dichromate. Titrations involving iodine.

Training Activity	Methodology	Related Competences (only degrees before RD 822/2021)	ECTS	Hours	As	Com	Description
Class Attendance (theory) [ON-SITE]	Lectures	CB02 CB03 CB05 E05 E14 G01 G03	1.12	28	N	N
Workshops or seminars [ON-SITE]	Workshops and Seminars	CB02 CB03 CB05 E14 G03 T04 T05 T06	0.4	10	N	N
Group tutoring sessions [ON-SITE]	Group tutoring sessions	CB02 CB03 CB05 E05 E14 G01 G03	0.08	2	N	N
Laboratory practice or sessions [ON-SITE]	Practical or hands-on activities	CB02 CB03 CB05 E14 E15 G03 T05 T09	0.64	16	Y	Y
Practicum and practical activities report writing or preparation [OFF-SITE]	Self-study	CB02 CB03 CB05 E14 G03 T04 T05 T06 T11	0.6	15	Y	Y
Progress test [ON-SITE]	Assessment tests	CB02 CB03 CB05 E05 E14 G01 G03 T04 T05	0.08	2	Y	N
Study and Exam Preparation [OFF-SITE]	Self-study	CB02 CB03 CB05 E14 G03 T04 T05 T06 T11	2.4	60	N	N
Final test [ON-SITE]	Assessment tests	CB02 CB03 CB05 E05 E14 G01 G03 T04 T05	0.08	2	Y	Y
Writing of reports or projects [OFF-SITE]	Self-study	CB03 CB05 E14 G03 T04 T05 T06 T11	0.6	15	Y	N
Total:			6	150
Total credits of in-class work: 2.4			Total class time hours: 60
Total credits of out of class work: 3.6			Total hours of out of class work: 90

As: Assessable training activity
Com: Training activity of compulsory overcoming (It will be essential to overcome both continuous and non-continuous assessment).

Evaluation System	Continuous assessment	Non-continuous evaluation *	Description
Laboratory sessions	15.00%	15.00%	The evaluation will take into account the work done during the laboratory practices sessions and the reports presented from each practice It is necessary to obtain a grade of 5 out of 10 to pass the course. If this is not achieved, a specific test will have to be carried out in the ordinary and / or extraordinary exame. The laboratory sessions are of compulsory attendance
Progress Tests	80.00%	0.00%	Two written assessment test that will consist of solving theoretical, theoretical-practical questions and numerical / analytical problems from lessons 1 to 3 and 4 to 6 respectevely. If the grade obtained in this test is higher than 6, you only have to examine from lessons 4 to 6 in the final test.
Final test	0.00%	85.00%	The final test will only be done by students who have not passed the progress tests or who want to improve their grade The final test will consist of solving theoretical, theoretical-practical questions and numerical / analytical problems for the entire subject. In this case the assessment of this exam will be 80% It is necessary to obtain a minimum grade of 5, to be able to compute it with the rest of the activities.
Assessment of problem solving and/or case studies	5.00%	0.00%	The student will be asked to deliver solved exercises, solve different issues related to the subject, solve practical cases
Total:	100.00%	100.00%

Not related to the syllabus/contents
Hours	hours
Group tutoring sessions [PRESENCIAL][Group tutoring sessions]	2
Laboratory practice or sessions [PRESENCIAL][Practical or hands-on activities]	16
Practicum and practical activities report writing or preparation [AUTÓNOMA][Self-study]	15
Progress test [PRESENCIAL][Assessment tests]	2
Study and Exam Preparation [AUTÓNOMA][Self-study]	60
Final test [PRESENCIAL][Assessment tests]	2
Writing of reports or projects [AUTÓNOMA][Self-study]	15

Unit 1 (de 6): INTRODUCTION. Classical techniques: Gravimetry and Titrimetry. Classification of volumetric methods. Primary standards
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	2

Unit 2 (de 6): ACID- BASE TITRATIONS. Acid-base Indicators. Types of indicators. Titration curves: Titration of monoprotic and polyprotic protolytes. Analytical applications.
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	8
Workshops or seminars [PRESENCIAL][Workshops and Seminars]	3

Unit 3 (de 6): COMPLEXATION TITRATIONS. Complexation reactions. Titration curves. Complexometric EDTA Titrations. Metallochromic indicators. Types of complexation titration. Applications.
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	5
Workshops or seminars [PRESENCIAL][Workshops and Seminars]	2

Unit 4 (de 6): PRECIPITATION TITRATIONS. Introduction. Titration Curves. Mohr¿ method. Volhard¿ method. Fajans¿ method. Most used primary standards
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	2
Workshops or seminars [PRESENCIAL][Workshops and Seminars]	1

Unit 5 (de 6): Gravimetry. Introduction. Types of gravimetric methods. Formation and treatment of precipitates. Precipitation gravimetry. General steps involved in gravimetric analysis.
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	3
Workshops or seminars [PRESENCIAL][Workshops and Seminars]	1

Unit 6 (de 6): REDOX TITRATIONS. Titration Curves. Redox indicators. Pre-treatment in redox titrations. Titrations with permanganate. Titrations with dichromate. Titrations involving iodine.
Activities	Hours
Class Attendance (theory) [PRESENCIAL][Lectures]	8
Workshops or seminars [PRESENCIAL][Workshops and Seminars]	3

Global activity
Activities	hours

Author(s)	Title	Book/Journal	Citv	Publishing house	ISBN	Year	Description	Link	Catálogo biblioteca
D. Skoog, D. West y F. Holler	Fundamentos de Química Analítica			Reverté		1996
D.C.Harris	Análisis Químico Cuantitativo			Reverte	ISBN 13: 97884291722	2003
D.C.Harris	Quantitative Chemical Analysis			McMillan	9781319154141	2015
G.D CHristian, P.K.DasGupta and K.A. Schug	Analytical Chemistry			Willey	978-0471214724	2014
M. Silva y J. Barbosa	Equilibrios Iónicos y sus Aplicaciones Analíticas		Madrid	Síntesis		2002
P. Hadjiidannou, G. Christian, C. Efstathion, D. Nikolelis	Problem Solving in Analytical Chemistry		London	Pergamon Press		1988
P. Yáñez-Sedeño, J. M. Pingarrón, F. J. Manuel de Villena	Problemas resueltos de Química Analítica			Sintesis		2003